Post 432344 (missing)
(geezmeister: "pseudo precipitation technique", Stimulants) ,………… Doing it will remove residual gaks and if not getting it completely clean, should get it clean enough for a successful RNX. (As the world of Gak-ta-lak, changes rapidly, this may in the future become untrue)You left the water reagent out of the ratio instructions entirely, when preceding you give some indication to the newbee of it's vitality without going in to any great detail.
H2o will be covered under cook times and temps, as they are inter related. Part one was covering preparation. As water isn't pre-prepared it was not included.
If you read one thoroughly beforehand it'll bee much easier.
S/D has been dreaming for nearly ten years now, and has been at the Hive for three. He tallys up with 1,156 posts.
So where's all of your write-ups Mr.halfkast?
Hmm, Oh, I see you're just a critic,......mmmmm?
No condensor
- Balloons as a first line of defense against hot strongly acidic gases,
I think that even critics should learn to read ;
It will work, stand alone, on top of a condenser, or with a P/P(attach P/P hose in place of punch-ball)
I've seen the information you just offered in a multitude of posts.
Might you reference some of them for us please.
So are you saying my criticism is wrong?
No, what I said what credentials do you have?
Why don't you focus more on learning chemistry instead of adding to this artwork
So, here’s the deal. All ratios given by experienced bees are correct. Now, you’re even more confused, huh? S/D will explain.
The standard ratios by the book, using L/G precursors are 1: 1: .3(1/3) E:I:R
Using MB/RP this should be adjusted to 1:1:1
Next we only need to know one simple fact. That is; It is not possible to over-reduce, pfed, using the REI method.
This means that any ratios that the “R” and “I” are higher (than the book ),are acceptable.
What do you call this?
Most chemistry books that I have seen include pictures.
If you could comprehend, you would have read the tiltle of this thread.
Where did you see, “Advanced details of REI RNX”????
Note, S/D from this point will no longer waste his time responding to the posts of those who have no information to offer, so instead choose to waste bandwidth.
Basically, I wouldn't bet my life on a balloon, and I definetly wouldn't burden a balloon with the responsibility of raising the pressure inside this type of environment to increase the concentration of the HI.
Post 28988 (missing)
(simonsays7: "Home made reflux condenser", Chemicals & Equipment)Why not use some copper tubing from an old cooler or the hardware store
You go right ahead and do that. If S/D was you he’d make out a will first, however.
It does not really matter what setup you use. All you're looking to do is contain the smoke and keep some HI in the RNX vessel. You can stick the hose in your ass, (better to use your dogs ass), and it will get the job done.
S/D apologizes for his shitty camera.
Is this better??
(https://www.thevespiary.org/rhodium/Rhodium/hive/hiveboard/picproxie_docs/000450084-file_sdbm.gif)
the point I've been trying to make is simply that a condensor is easily made and easily kept cold for 12hrs. The balloon can bee kept on top.
ScottyDogg, thats horrifying that you'd go to the effort of preparing a large reaction like that without preparing the most basic of condensors.
beyond belief and reason.
The point we are trying to make is that its not necessary because a balloon is sufficient. Most of us have used a condenser, but unless your doing a long reflux then one is not necessary.
We know this because we have tried this both ways many times. Its called experience.