SUCCESS!!. Thermal rearrangment of the glycol oil worked just fine. Glycol oil was an antifreeze, see thru green. After heating to 260°C for 1 1/2 hours the glycol (now ketone) oil became darker, see thru brownish in color, heating mantle was turned down, time passed to cool down oil, then full vacumm was applied and an opaque yellowish green ketone came over at arounf 214°C Approximatley 25°-30° higher than the Isosafrole precursor.
. Thank you - thank you, no please, sit...sit please , applause isn't necessary!! No Really!
Cheese will work with 100gm of Isosafrole from now on. Not sure scaling this up too much is good for the Iso.??
Thanks to Vibrating Lights, Noj, Pickler, Chromic, PooBearForever, Psycokitty, Rhodium, Locrian, El_Zorro,sYnThOmAtIc and last but not least... The Big R. (Let's not forget Sasha, Strike, and all the mods on the Hive for making it possible.) This acceptance speech has got to end soon.......this ain't the academy awards
Cheeseboy-a whiteboy with Soul Like a black guy without soul
May The Source Bee With You Always.