Author Topic: hypo cook gone wrong  (Read 2401 times)

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NedKelly

  • Guest
hypo cook gone wrong
« on: December 17, 2003, 11:44:00 AM »

wareami

  • Guest
What have we learned?
« Reply #1 on: December 17, 2003, 02:17:00 PM »
We've learned that anybee can extract pfed with practice.
What they extract is reliant on the method chosen to extract said formulation or strength.
We've learned that OrangeII gaak cannot be detected with the naked eye in a pile of extracted E or pfed.
Tests performed prior to rxn SHOULD be a good indication of the feeds quality.
This is dependant on the testing method. And that is dependant on the detection experience of the tester.
Never assume that the bee before you doing the extraction is qualified or experienced enough to detect the tougher to detect inhibitors or denaturants.
The price to pay for the undersite will be the waittime it takes for the encapsulation effects to subside!
One to 3 daze depending on the amount!
Take Osmiums advice concerning the addition of an abundance of dh2o to the rxnsolution prior to basing and the amine won't become as trapped as it is when standard amounts of dh2o are added!
Bees will correct me if I'm wrong.
The only two frontside pfed extractions that address OrangeII Gaak are the tetratrap and the slanted egull(tetra and japandrier)


geezmeister

  • Guest
Too little information
« Reply #2 on: December 17, 2003, 03:59:00 PM »
You provide too little information to even guess what your problem is. Adding salt and tolly isn't going to extract any remaining pseudoephedrine. You would need to dilute the solution you have of psuedo, hypo, I2, and whatever else might be in there, base it to about pH12, then extract to a nonpolar solvent. That doesn't mean you will recover pseudo, or that you had pseudo to recover.

Ware overlooks the solvents boils with JD/MEK and JD/Naptha mixtures which also removes the orange II gak. He feels about the full cure method of cleaning like I feel about the egull--- we are on opposite sides of a fence on how we prefer to proceed to get clean pseudo. I like solvent boils and a/b extractions, he prefers tetra combos and alcohol.

One of us probably has had too much tequila at some point, but we can't decide which one of us it was.  ;D


placebo

  • Guest
1.) Whether you have pseudo or meth, you will...
« Reply #3 on: December 18, 2003, 06:28:00 AM »
1.) Whether you have pseudo or meth, you will need to basify it( NaOH) to get it to move into the toluene.

2.) Never react anything that you don't know personally is clean. Test it, vapourise on a bit of foil, check it's clean, or at least dissolve in methanol and recrystalise.