Would it be possible to chlorinate 2,5-dimethoxyamphetamine (t o yield DOC) with HCl in tert-butyl hydroperoxide as discussed in the following document: https://www.thevespiary.org/rhodium/Rhodium/chemistry/halosuccinimide.txt (https://www.thevespiary.org/rhodium/Rhodium/chemistry/halosuccinimide.txt)
?
I've searched all day, and the alternatives doesn't look that hot, rather avoid liquid chlorine and perchloric acid (NCS-route seemed like a simple procedure otherwise) if I could. :D
You posted about the Oxone/KCl procedure a while ago: Post 384324 (https://www.thevespiary.org/talk/index.php?topic=11530.msg38432400#msg38432400)
(Barium: "A little 2C-C perhaps", Novel Discourse)
Did you ever boost your yields?