This has never happened before, the gassing was going fine, then I took the rod out for a look and the crystals had turned to goop. It was my fault really as the toluene was quite warm and I was gassing way too quickly as I was in a hurry. Anyway, remedy, would that just be to dump some 5%HCl solution in, then freebase again, dry, and re-gas, albeit more slowly. Is the salt stable under these acidic conditions (that is such a stupid question but I don't really want to waste this so I will ask anyway)
Anyone had this happened before, or will the oil eventually crystallise???
ta
wacka wacka wacka