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Author Topic: DMSO autoxidation  (Read 4753 times)

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pablos

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DMSO autoxidation
« on: June 30, 2004, 04:38:00 AM »
Have anyone already tried the autoxidation of anethole with dmso?
The procedure papers give exellent yeld (77%) of ketone in only 8
hours at 120 grad.
I have 25 grams pure anethole at home and 100 ml dmso but I can´t find  the ratio in this papers  and I speak not japans.Any good idea?
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Rhodium

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We are not mind-readers.
« Reply #1 on: June 30, 2004, 05:04:00 AM »
We are not mind-readers. Use the post linking feature.

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pablos

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sorry
« Reply #2 on: June 30, 2004, 10:21:00 AM »
Sorry I tought it was a well known document.

https://www.thevespiary.org/rhodium/Rhodium/pdf/isosafrole.dmso.oxidation.pdf


this is the paper in japan
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