Author Topic: Isosafrole expoide stability  (Read 1773 times)

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Vibrating_Lights

  • Guest
Isosafrole expoide stability
« on: December 02, 2001, 04:57:00 AM »
Does any one know how stable the isosafrole epoxide is. Ie.  Can you keep it in the freezer for extended periods of time without decomposition.  I believe mabyee ritter said something about it a while back but a thourough search yeilded nothing.
VL_

Rhodium

  • Guest
Re: Isosafrole expoide stability
« Reply #1 on: December 02, 2001, 05:32:00 AM »
Ritter stored isosafrole glycol. But I think the pure distilled epoxide can last very long if cool, and protected from light and moisture.

uemura

  • Guest
Re: Isosafrole expoide stability
« Reply #2 on: December 02, 2001, 09:54:00 AM »
Vibrating_Lights!
the only thing Uemura can tell is that his anethole expoxide was water clean after destillation but now got a very light yellow touch. Epoxide is stored in a clear glas bottle at room temp. Should put the stuff into the freezer.  :)  Or work it up....

Vibrating_Lights

  • Guest
Re: Isosafrole expoide stability
« Reply #3 on: December 02, 2001, 10:01:00 AM »
Wouldn't it be great to make a big chunk of epoxide at one time and just keep it in the freezer.  then when ever was nescesary be only 7 hrs from crystals.