The Vespiary

The Hive => Stimulants => Topic started by: GC_MS on April 10, 2003, 12:45:00 AM

Title: Ephedrine Compilation
Post by: GC_MS on April 10, 2003, 12:45:00 AM
Brian T. Schaneberg, Sara Crockett, Erdal Bedir and Ikhlas A. Khan. The role of chemical fingerprinting: application to Ephedra. Phytochemistry 62(6) (2003) 911-918

Abstract - Ephedra sinica ,known as Ma Huang ,is one of the oldest medicinal herbs in Traditional Chinese Medicine (TCM).Preparations, namely teas,of E.sinica have been used for over 5000 years as a stimulant and as an antiasthmatic.In the West, extracts of E.sinica, E. intermedia or E. equisetina are most commonly used in dietary supplements as a stimulant and to promote weight loss. More than 50 species of Ephedra are native to both hemispheres, but the detection of ephedrine alkaloids has been limited to species in Eurasia. Currently, methods exist to quantitate the ephedrine alkaloids in extracts of plant material or dietary supplements, but the methods are not able to verify the extract is of an Ephedra species. Reverse phase high performance liquid chromatography with photodiode array detection was applied for the chemical fingerprinting of the Ephedra species.Two regions of comparison were determined in the chromatograms at 320 nm. The series of peaks between 52 and 64 min confirms an Ephedra species is being analyzed. The aforementioned peaks also could distinguish between Ephedra species from Eurasia, North America and South America. Peaks at ca. 57 and 59 min were isolated and determined to be two new compounds,4-(2-eicosyloxycarbonylvinyl)-benzoic acid and 4-(2-docosyloxycarbonyl-vinyl)-benzoic acid respectively. Authentication of ground plant material as Ephedra can be achieved by this chemical fingerprinting method.

DOI:

10.1016/S0031-9422(02)00716-1 (http://dx.doi.org/10.1016/S0031%2D9422%2802%2900716%2D1)



Title: Phytochemistry 62(6) (2003) 911-918
Post by: Rhodium on April 15, 2003, 04:08:00 PM

Phytochemistry 62(6) (2003) 911-918 (https://www.thevespiary.org/rhodium/Rhodium/pdf/ephedra.chemical.fingerprinting.pdf)

(https://www.thevespiary.org/rhodium/Rhodium/pdf/ephedra.chemical.fingerprinting.pdf)
Title: damaged file
Post by: mickyfinn on September 07, 2003, 03:54:00 PM
Tried to d/l the file and recieved an error stating it could not be repaired.
Title: Re: Damaged link....
Post by: java on September 09, 2003, 10:40:00 AM
Try pasting this on the address window of your browser.....

https://www.thevespiary.org/rhodium/Rhodium/pdf/ephedra.chemical.fingerprinting.pdf (https://www.thevespiary.org/rhodium/Rhodium/pdf/ephedra.chemical.fingerprinting.pdf)



Title: file damaged error must be local
Post by: mickyfinn on September 09, 2003, 06:35:00 PM
Thanks java...unfortunately I get the same error message...plus a new error on connect using just the link...I'll look into reinstalling acrobat.
Title: Have you tried...
Post by: SHORTY on September 09, 2003, 11:43:00 PM
Have you tried right clicking the shortcut and choosing

"save target as"?

Even if you don't have acrobat installed you should still bee able to download the file.

Title: It should work now
Post by: Rhodium on September 15, 2003, 10:29:00 AM
I have re-uploaded the file now, and it works for me. If it still doesn't work for you, try installing the latest version of

Adobe Acrobat (http://www.adobe.com/products/acrobat/readstep2.html)

(http://www.adobe.com/products/acrobat/readstep2.html).