Post 443814 (https://www.thevespiary.org/talk/index.php?topic=11751.msg44381400#msg44381400)
(Lego: "P2Pol from toluene and ethanol", Novel Discourse)
To follow would simply be a RA using Al/Hg and MeAm? What amine does it produce?
Meth of course. SWIM isn't talking about aminating the alcohol, but doing a jones oxidation (or whatever) or something similar to strip off that hydrogen. Nothing but ketone left from that my friend.
Post 27112 (missing)
(firecracker: "TLC tutorials?", Chemistry Discourse)Post 212345 (missing)
(catastrophe: "Purity Tests via TLC", Newbee Forum)Post 432737 (https://www.thevespiary.org/talk/index.php?topic=9108.msg43273700#msg43273700)
(ClearLight: "Making your own TLC Standards", Methods Discourse)Post 432209 (https://www.thevespiary.org/talk/index.php?topic=8834.msg43220900#msg43220900)
(ClearLight: "Question on Hard Layer TLC Binders", Methods Discourse)Post 401159 (https://www.thevespiary.org/talk/index.php?topic=6684.msg40115900#msg40115900)
(TheBlindGenius: "Using TLC for quantitative analysis", Chemistry Discourse)Post 380759 (missing)
(MaDMAx: "Chromatography basics and TLC", Newbee Forum)https://www.thevespiary.org/rhodium/Rhodium/chemistry/psilo-tlc.txt (https://www.thevespiary.org/rhodium/Rhodium/chemistry/psilo-tlc.txt)
Post 108792 (missing)
(dormouse: "Lab Suggestions -ymir", Novel Discourse)Post 304601 (https://www.thevespiary.org/talk/index.php?topic=9388.msg30460100#msg30460100)
(Rhodium: "Zubrick TLC Chapter", Methods Discourse)Post 304827 (https://www.thevespiary.org/talk/index.php?topic=9388.msg30482700#msg30482700)
(LaBTop: "Ahumm,", Methods Discourse)Post 347588 (https://www.thevespiary.org/talk/index.php?topic=9388.msg34758800#msg34758800)
(ClearLight: "column and plate preparation", Methods Discourse)
A-
try saturated aqueous bisufite solution.
Well, hate to be an asshole, but no shit! SWIM would have if SWIM had some bisulfite.
SWIM tried comlpexing it with KI but it didn't work (as far as SWIM can tell). Eventually, SWIM just said "fuck it" and poured it down the sink. SWIMS gonna try this again probably starting tomorrow. This sucks that SWIM is broke and can't afford a MV yet. The sun sucks ass (esp. when it rains at least once a day here).
Also, this time SWIM is gonna have it in a pyrex erlenmeyer with glass stopper, instead of the pyrex beaker covered with aluminum foil. SWIM beleived the evaporation of the acetone severly hindered this reaction. Didn't think about it like SWIM should first off.