The Vespiary

The Hive => Newbee Forum => Topic started by: pink_dust_angel on July 28, 2004, 12:49:00 PM

Title: benzyl chloride synth
Post by: pink_dust_angel on July 28, 2004, 12:49:00 PM
in benzyl chloride synth on rhodiums site how concentrated doesthe HCl have to be?
Title: Details, please
Post by: Rhodium on July 28, 2004, 02:03:00 PM
Provide a link and tell us exactly which preparation you are referring to - there are several benzyl chloride syntheses on my page.

Title: i am talking about https://www.rhodium.ws/chemi...
Post by: pink_dust_angel on July 28, 2004, 05:51:00 PM
i am talking about

https://www.thevespiary.org/rhodium/Rhodium/chemistry/benzylchloride.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/benzylchloride.html)


its the synth that says "Chlorination of benzyl alcohol with conc. HCl "
Title: 10-12 mol/L
Post by: Rhodium on July 28, 2004, 05:58:00 PM
The stronger acid you use, the higher your yields will be. Concentrated 36-37% HCl is the best to use, but you might get away with using the 31% strength too, just compensate by using a larger excess of acid.