I haven't found that method mentioned on rhodium or elsewhere, but there is a US patent 2806033 that describes how to demethylate oxycodone by boiling with concd hydrobromic acid. I couldn't find the full patent text, does anyone know how that method works and at what yields?
Thanks,
Slow your speech and lower the pitch of your voice.
http://l2.espacenet.com/espacenet/bnsviewer?CY=gb&LG=en&DB=EPD&PN=US2806033&ID=US+++2806033A1+I+ (http://l2.espacenet.com/espacenet/bnsviewer?CY=gb&LG=en&DB=EPD&PN=US2806033&ID=US+++2806033A1+I+)
The above post is purely fictional. Any resemblance to "real-life" is purely coincidental.
Thanks. Well, it looks like Epikur's mthod at rhodium has a much better yield.
Slow your speech and lower the pitch of your voice.