The Vespiary

The Hive => Stimulants => Topic started by: DarkSky on December 10, 2003, 06:39:00 PM

Title: Opps, grabbed the wrong can!
Post by: DarkSky on December 10, 2003, 06:39:00 PM

Title: Is it possible to take the soultion, wash with
Post by: DarkSky on December 10, 2003, 07:15:00 PM

Title: Let the acetone evaporate
Post by: jackhole on December 10, 2003, 08:12:00 PM

Let the acetone evaporate and proceed as usual.  With a reaction that size, it should only take a few hours.

Title: Good advice...
Post by: energizer_bunny on December 11, 2003, 09:58:00 AM

Evap off the tone then do the wash...but!

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All this was cooked on 99.5C for 3 hours and everything was going perfect.

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Where is it written that a rxn under LongWetReflux conditions is going to be complete @ 3hours?
That calculation defy's scientific logic.