The Vespiary

The Hive => Methods Discourse => Topic started by: TripleXtacy on September 19, 2001, 10:01:00 AM

Title: Aniline synth???
Post by: TripleXtacy on September 19, 2001, 10:01:00 AM
A friend of swims who likes to play with fentanyl, has recently encountered a stumbling block. Due to new obstacles recently imposed in his area in regards to acquisitions of aniline have led him to discover new methods of possession.
His question is, has anyone experimented with the production of aniline via hydrogenation of nytrobenzene with Iron turnings/fillings?
If not has anyone got any tips as he is ready to give it a try anyways.
Thanks for your time.

The only secrets are the ones that keep themselves.
Title: Re: Aniline synth???
Post by: Rhodium on September 19, 2001, 10:06:00 AM
Yes, and it is an easy reduction. Look in the file

https://www.thevespiary.org/rhodium/Rhodium/chemistry/quaalude.txt (https://www.thevespiary.org/rhodium/Rhodium/chemistry/quaalude.txt)

for general directions.
Title: That text doc was HTMLized to http://www.rhodium.
Post by: Bwiti on June 05, 2002, 01:41:00 AM
That text doc was HTMLized to

https://www.thevespiary.org/rhodium/Rhodium/chemistry/quaalude.cheapskate.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/quaalude.cheapskate.html)

8)

Love my country, fear my government.
Title: Yup, 300 documents HTMLized so far, 100 to go.
Post by: Rhodium on June 05, 2002, 01:46:00 AM
Yup, 300 documents HTMLized so far, 100 to go.
Title: Aniline
Post by: PrimoPyro on June 05, 2002, 01:49:00 AM
Can also be made by reaction of benzamide with hypochlorite salts. Another easy reaction, and Cheapskate used the same principle for his Anthranilic acid synthesis, from phthalic acid.

                                                    PrimoPyro
Title: From what I remember the process in J. Gen. Chem.
Post by: PolytheneSam on June 05, 2002, 03:15:00 AM
From what I remember the process in J. Gen. Chem. is electrochemical. 

Post 199874 (missing)

(PolytheneSam: "Re: Oxidative amination of an alkene, maybe an electro possiblity.", Chemistry Discourse)


http://www.geocities.com/dritte123/PSPF.html
The hardest thing to explain is the obvious
Title: very easy
Post by: hellman on June 19, 2002, 03:10:00 AM
Benzene-nitrobenzene`````h2so4
nitrobenzene-anilin''''''zn/hcl or sn/hcl
If you want the procedure step by step just ask,.
It is also from vogels pract