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21
News / Re: Smoking Toad Venom Phenomenon: Hamilton's Pharmacopeia Season 3
« Last post by carl on January 05, 2021, 10:37:18 PM »
*cough cough*
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Quote
100 grams of 5-MeO-tryptamine freebase is dissolved in MeOH with vigorous magnetic stirring. A thermometer probe is inserted into the methanolic 5-MeO-tryptamine, and the solution is cooled until it nears 0 °C. Aq. KOH is used to dissolve and stabilize 100 grams of NaBH4, and the solution is transferred into an addition funnel. A second addition funnel is charged with a MeOH-stabilized aq. 37% formaldehyde solution, and the drop-wise addition begins. "And now I start adding the borohydride." [...] Borate salts gradually precipitate, and the salt volume is reduced by overnight heating. As the methanol evaporates, 5-MeO-DMT precipitates as a brown oil and coalesces on the surface. "Pretty beautiful." Simple distillation is used to strip the remaining water, followed by purification of the crude freebase via short path vacuum distillation, "We did it. Yes.", and recrystallization. [...] After TLC had shown total transformation of the starting material, LC-MS confirmed the product was 5-MeO-DMT.

There sadly is some stuff missing in that synthesis, first of all if he uses Acetone/dry ice as his bath, then the reaction most likely will run below 0°C. Doesn't mention reaction time or amount of HCHO. Simple distillation may or may not carry along freebase 5-MeO-DMT. Also a bit puzzled how he can reduce salt volume by heating, probably meant to say solvent volume.
Not the most efficient or clever workup, but if it works, it's not stupid, right? ;)
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News / Re: Smoking Toad Venom Phenomenon: Hamilton's Pharmacopeia Season 3
« Last post by Sawdust and Honey on January 03, 2021, 05:34:32 PM »
Has anyone been able to scan the pamphlet and share it? I wanted to buy it myself, but it's already sold out.
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Harm Reduction Resources / Re: Be open about drug use
« Last post by arkoma on January 03, 2021, 11:43:09 AM »
It all depends (openness about use of dope) on WHERE, WHEN and WHOM you live/work/exist/do drugs with.  Where I'm at now in my life, I'm pretty fucking "flat-spoken" (in other words don't ask if you don't want to know), but I'm a small, small town where everyone knows me and knows I'm not a thief or a "reseller". I'm the village eccentric...........

If your young, raising kids yada yada yada, yeah, ya better be cautious as hell about who you let know your business.  Just sayin'.....

*edit* Been using meth off and on (more on than off) for forty years and I damn sure still go outside in the daytime......LMFAO
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Harm Reduction Resources / Re: Be open about drug use
« Last post by Kasey Jones on January 02, 2021, 10:12:19 PM »
I believe that it's true only for opiates. They make you isolate from the society for sure, but that's their action profile, I believe. And they're perfect for IV use, hence why most drugs applied IV are opiates.

I doubt that other groups of drugs are like that. For example amphetamine or cocaine. Do they make you isolate from the society? I don't think so!

I hate treating all different drugs in the same manner as opiates! They're something beyond, the true evil and treating all different drugs in the same manner as opiates, leads to huge misunderstanding and majority of the tabu, or myths about drugs, which makes drug politics just miserable.


Coke use starts as lines at a party. Then it's a private party. Then a few other trusted friends. Then one other person.  Then its just and your coke, especially if you are shooting it as it makes you so.paranoid that between shots you spend your time tiptoeing around the house and peeking out the window.  If you get high enough you will hear things that aren't there.  Granted it takes a long time to get to that level and usually only after you've graduated to IV.  I was warned by older users not to make the.jump away from snorting since once you've tasted that rush, everything else is a tease: you can't feel satisfied unless you hear the world crushed like an aluminum can and tunnel vision as the train comes breezing by.  It's all at once terrifying and exhilarating and the more you do it,you push the line to see how far you can go. It reminds me of the character Frank.from Hellraiser:  you think you'd been to.the highest highs but near death theres a secret place that you get a fleeting glimpse of as you clutch your arm and try and relax while the world is spinning...I imagine the cynobytes about to appear...
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News / Re: GMP Mdma is made from Heli :)
« Last post by Zippy on January 01, 2021, 08:14:29 PM »
Safrole is used in the perfumery industry as well so they may have used that.

I have done GMP synthesis. Lots of paperwork, batch records, oh hey is your scale in spec for recent calibration? how about the weight you use to check it are those ok and within date?  Oh you wanted to bring in a spatula that's not on the equipment list well we need to attach a DWP (Deviation from Written Procedure) then it all needs to be signed countersigned passed by QA and QC, then it can be released. Maybe.
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News / Re: GMP Mdma is made from Heli :)
« Last post by carl on January 01, 2021, 11:47:01 AM »
Its not 84% pure, damn! 84% of MDMA HCl are MDMA, the rest is the HCl ion ::)
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News / Re: GMP Mdma is made from Heli :)
« Last post by foroz on January 01, 2021, 05:29:57 AM »
https://www.theguardian.com/society/2016/sep/16/mdma-ptsd-therapy-trauma-maps-medical-study

Quote
1kg of MDMA – worth close to £300,000 ($398,000).


Jesus, they're getting ripped off...    ::)





/CJ

and they always will my friend hence why we should only help legalization and not hinder it.

when its legal its just a slap on the wrist for us but the money will still be there :)

got to love capitalism  8)
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News / Re: GMP Mdma is made from Heli :)
« Last post by Shy Guy on January 01, 2021, 04:58:36 AM »

I wonder what gets it from 84% to 99.95 in powder form

distilled MDP2P (from piperonal) + Al/Hg Reduction with Toluene extraction and some washing (fb not distilled) + A single recrystallization = pristine white crystals

...but with a disappointing purity of 90%

Same process for P2P from benzaldehyde resulted in 99.54% purity. All tested in Spain.
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Harm Reduction Resources / Re: Be open about drug use
« Last post by spice on December 31, 2020, 04:25:00 AM »
i piss alone, ugh hoh
i don't want nobody to know
that i don't have the pressure of some of the other boys
they make a noise, it scares me so
i piss alone, alone
i don't want nobody to know
that i don't have the pressure of some of the other boys
leave me alone, alone
i just want to be on my own
'cause i haven't got the pressure of some of the other boys
i want a world where pissing troughs are obselete
there's only rows and rows of cubicles
i'm so afraid
when i try it is often delayed
i stand and stare into the air
and then i might just put it away
so quiet in here
the only sound around is the fear
the other guy is pounding the wall
like he's shooting dear
i need a place where i can close and lock the door
there i can stop and let it flow

regurgitator I piss alone

I trip alone as well  ;D

LOL

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