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Preparation of LSD with Thionyl Chloride

Started by Protium, January 15, 2003, 11:02:00 PM

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Rhodium

It was actually lugh who retrieved the article, I just hosted it.

You have gotten it all wrong, they say they are condensing the structure IX with the hydrochloride salt of lysergic acid chloride using chloroform/tributylamine as solvent. There are also talk about making the acid chloride with oxalyl chloride and then something about making the acylazide with NaN3 - some german bee migh shed some light on this.