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Is there any downside when i do not distill

Started by pirat, April 18, 2003, 05:58:00 PM

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pirat

buffered performic
bisulfite addition and recovering à la eleusis without distillation of the ketone!!
al/hg nitro
mdma
this really works

Is there any downside when i do not distill the ketone??

Antibody2

bisulfite  often yeilds gooey crystals that are not really pure, these impurities carry over into subsequent rxns reducing yeild, causing side reactions and complicating further purification. but it can work to some extent

take the search engine out for a test drive there is plenty already posted on the subject