I have OCRed or transcribed the following list of journal articles, books and notes.
3855306.doc
US pat 3855306, Pius Anton Wehrli, Hoffmann-La Roche Inc., Issued: Dec. 17, 1974.
Abstract: Process for the preparation of 3,4,5-trimethoxybenzaldehyde from vanillin comprising the steps of bromination, hydrolysis and methylation.
4,731,482.doc
US Pat 4,731,482 (from Rhodium), Process For The Preparation Of Phenylpropanones, Carlo Vanturello et al. - allylbenzenes are catalytically epoxidized by H2O2, in a biphase system comprising an aq. phase containing H2O2 and an organic phase containing: allylbenzene, a solvent, a catalyst having formula (Quat.)3PW4O24. The epoxide is hydrolysed to P2P with LiI.
Acetamide.doc
1. Acetamide; Coleman & Alvaram; Org. Syn. vol. III, 1923, p3 & Org. Syn. Coll. vol. I, p3;
2. Chloro-acetamide (Acetamide, ?-chloro-) Jacobs & Heidelberger; Org. Syn. Coll. vol. 1 p 153.
3. The Preparation of Acetamide; Rosanoff, Gulick, & Larkin; JACS 33, 974-77, 1911.
Allyl-ben.doc
Hydroxide Ion Initiated Reactions under Phase-Transfer-Catalysis Conditions. 5. Isomerization of Allylbenzene via Hydroxide Ion Extraction; Mere Halpern, Yoel Sasson and Mordecai Rabinovitz;
J. Org. Chem. 1983, 48, 1022-1025
US Patent 3,852,305; To: Nagase; Tsuneyuki, et. al.; Date: 3/12/74: Isomerization of Alkenyl-Alkoxybenzenes
Allylcat.doc
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The Behaviour of Allyl Derivatives of Catechol & Resorcinol Toward Heat, By Charles D. Hurd, Harry Greengard and Forrest D. Pilgrim; JACS 52, 1700 (1930)
Amino-a.doc
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The Action of Formaldehyde on Amines and Amino Acids; By H. T. Clarke, H. B. Gillespie & S. Z. Weisshaus; JACS 55, 4571-4587, Nov. 1933.
CA-dealk.DOC
CA 4809(7), (1942). - Cleavage of phenol ethers with pyridine hydrochloride. Vinzenz Prey. Ber. 74B, 1219-25 (1941). - with pyridine.HCl
CA: 44, 5909b (1950): Dealkylating alkoxy aromatic amines. Curt G. Vogt and Franz Marschall (to General Aniline & Film Corp.). U.S. 2,497,248, Feb. 14, 1950. - with AlCl3 and a base.
Chemical Abstracts, CA:52, 6255h, (1958) Selective cleavage of ethers by aluminum chloride. Cs. Szántay (Tech. Univ., Budapest). Acta Chim. Acad. Sci. Hung. 12, 83-91(1957).
CA 45, 7089 b, (1951) - Dealkylation of ?-(2-alkoxy-1-naphthoyl)propionic. S. I. Sergievskaya and A. A. Chemerisskaya (S. Ordzhonikidze All-Union Chem.-Pharm. Inst., Moscow). Zhur. Obshchei Khim. (J. Gen. Chem.) 20, 2284-8 (1950). Heating 5 hrs. with AlCl3
CA 55:21578i (1961) - Decomposition of lignin. 1. Action of compounds of the type RNH1-3X. Donald H. Grangaard (Kimberly-Clark Corp., Neenah, Wis.). Tappi 44, 433-9 (1961).
Catechol.doc
Preparation of Catechol: H. D. Dakin; Org. Syn., coll. vol. 1, p 148.
Chem-abs.doc
Constitution of ephedrine. Desoxyephedrine. A. OGATA; CA 14:745 (1920) J. Pharm. Soc. Japan 451, 751-64 (1919).
CA 56:9714 (1962); New method of prepn. of heliotropin (I) by condensation of methylene ether of pyrocatechol (II) with formaldehyde (III) in the presence of m-nitrobenzene-sulfonic acid (IV), Al (V), and hydrochloric acid was described. Tr. Vses. Nauchn.-Issled. lnst. Sintetich. i Natural'n Dushistykh Veshchestv 1961, No. 5, 21-5.; E. D. Laskina, T. A. Devitskaya, Z. N. Bychkova, R. F. Shilina, and T. V. Sukhorukova.
Selective cleavage of ethers by aluminium chloride, Cs. Szántay (Tech. Univ., Budapest).
CA 52:6255 (1958). Acta Chim. Acad. Sci. Hung. 12, 83-91 (1957).
Synthesis in the 1,2-methylenedioxybenzene series (safrole, piperonal, and piperine); Claude Feugeas (Lab. Syn. Organ., Paris); CA 61:16001a (1964); Bull. Soc. Chim. France 1964(
, 1892-5 (Fr.).
Heliotropin synthesis from pyrocatechol through the pyrocatechol aldehyde; V. N. Eliseeva and T. A. Devitskaya; CA 54:1391 (1960); Trudy Vsesoyuz. Nauch. Issledovatel. Inst. Sintel. i Natural. Dushistykh Veshchestv 1958, No. 4, 31-4.
Veratryl chloride and cyanide. F. Dengel (to Knoll A.-G. Chemische Fabriken); CA 49:15963a (1955); U.S. 2,695,319, Nov. 23, 1954. - Chloromethylation of veratrole(I) in ~ 70% yield.
Preparation of aromatic aldehydes by the "nitroso" method. V. N. Eliseeva and T. A. Devitskaya.
CA 51:7326c (1957); Zhur. Priklad. Khim. 29, 1894-6(1956). MeOPh --> 44% anisaldehyde
Synthesis, structure, and transformations of ?-(2-ethoxy-1(6)-naphthoyl)-propionic acids. S. I. Sergievskaya, A. V. Danilova, and A. A. Chemerisskaya (S. Ordzhonikidze All-Union Chem.-Pharm. Inst., Moscow). CA 45:7089e (1951); Zhur. Obshchei Khim. (J. Gen. Chem.) 20, 2314-20 (1950).
Dealkylating alkoxy aromatic amines. Curt G. Vogt and Franz Marshall (to General Aniline & Film Corp.). CA 44:5909 (1950); U.S. 2,497,248, Feb. 14, 1950. An increased yield of hydroxylated aromatic amine is obtained when alkoxy aromatic amine salts are dealkylated with an Al halide at elevated temps. in an inert org. solvent.
?-Methyl-3,4-methylenedioxyphenethylamine. Ichiro Hirao (to Ono Drug Industries Co.). CA 48:2097b (1954); Japan. 1770 (1952), May 20. Piperonal + ethyne + 20 atm. --> 1-(HO)-(MDP-2-P)
Preparation of 1,N-diveratrylethylamine and 1,N-dipiperonyl-ethylamine. Stanislaw Biniecki. Eugeniusz Muszynski, Helena Jagiellowicz, and Zdzislawa Chojnacka (Akad. Med., Warsaw). CA 58:3334 (1963); Acta Polon. Pharm. 19, 31-5 (1962). Veratraldehyde, EtNO2, and BuNH2,(cat).
Derivatives of amphetamine. E. Muszynski (Akad. Med.. Warsaw). CA 58:3334 (1963); Acta Polon. Pharm. 18, 471-8 (1961) (in Polish). Safrole and 0.1 g. HgCl2 in 5 vols. AcOH was satd. with HBr. left 2 days at 0o, neutralized with NaHCO3, extd. with Et2O, and distd. to give 73.3% MDP2-bromopropane (I), b15 162-5o. nD16 1.5628.
Volatile oil of Cinnamomum kanahirai Hayata or "shoggu" oil. I. Constituents of root oil. Tetsusaku Ikeda and Tsutomu Naito. CA 32:86969 (1938); J. Chem. Soc. Japan 59, 213-23 (1938).
Essential oil of pha-chiun. II. Tetusaku Ikeda, Syozaburo Takeda, Hatuo Nakama and Tyuzi Yokohara.
CA 36:6753 (1942); J. Chem. Soc. Japan 61, 583-91 (1940); cf. CA. 25:3438. Detailed composition of Camphor tree oil.
Saturated carbonyl compounds from unsaturated hydrocarbons. Japan Oil Co. Ltd. CA 64:3358f (1966); Brit., 1,008,923 (C1. C 07c), Nov. 3, 1965; Japan. Appl. May 25, 1963; 6 pp. Carbonyl compds. are formed by oxidn. of unsatd. hydrocarbons using Hg(NO3)2 in HNO3 as the oxidizing agent.
Chemistry.doc - missing
Oxidation of terminal alkenes to methyl ketones using Palladium cat.; (Wacker) Tsuji, Synthesis 1984, 371
Phase transfer cleavage of phenolic ether Using HBr & surfactant; Landini, Montanari, Rolla, Synthesis, 1978, 771
Cleavage of Ethers with Aqueous HCl in the presence of Surfactants; B Jursic, J Chem Research (S), 1989, 284-5.
2-nitropropenylbenzene. Amphetamine, or P2P from propenyl benzene; J. Prakt. Chem. 137, 345; 138, 271 (1933); JACS 54, 273 (1932)
Methylamine from formalin and NH4Cl
Piperonyl acetone from isosafrole; CA 49:10958i, T Fugisawa, Y Deguchi.
J. Pharm. Soc. Jpn. 74, 975-7, 1954
Reductive animation of Ketones using iron pentacorbonyl.
Watanabe et al, Tetrahedron Lett. 22, 1879, 1974
Watanabe et al, Chemistry Lett. 1974, 1265.
Extraction of Urea from urine: (Sheerwood Taylor, 311) - for the truly desperate!
Extraction of Eugenol from cloves (2); Experimental Organic Chemistry; Durst, Gokel, Durst, Gokel; McGraw Hill; 1980; p. 467.
Cinnamom.doc
The Cinnamomum Species in China: Resources for the Present and Future; Perfumer & Flavorist, vol. 19(4). July/August 1994 p17.
Cl-89.doc
An Efficient Method for the Hofmann Degradation of Amides by Use of Benzyltrimethyl-ammonium tribromide, Chemistry Letters, pp. 463-464, 1989, The Chemical Society of Japan; S Kajigaeshi, K Asano, S Fujisaki, T Kakinami, T Okamoto
Claisen.doc
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Claisen rearrangement. Chemical Reviews 27, 495, 1940, D S Tarbell
Prep. of allyl aryl ether ref: JACS 62, 771, 1940, Smith, Hoeln, Whitney
Use of Nickel bis[acetylacetone] catalyst, NaHCO3 as HCl acceptor. Synthesis 1982, 186-188, Camps, Coll, Moreto
Notes on Guaicol
Claviceps paspali.doc
Claviceps paspali, Nov. 27, 1916 p 403.
CA 90: 118108c Production of ergot alkaloids of lysergic acid derivatives (LAD) by submerged fermentation. Sastry, Ojha & Atal. Indian Drugs 1979 16(4), 88-93 (English).
69349d Ergotamine and ergocryptine production. Societa Farmaceutici Italia. Brit. 1,158,380 (Cl. C 07d, C 12d), 16 pp.
69351y Lysergic acid and its derivatives by fermentation.
Cleavage.doc
Cleavage of the methylenedioxy group. Ernst Spath and Herbert Quietenstsky. Ber. 60B, 1882-90; (1927); Chemical Abstracts Vol. 22, page 86.
Dakin.doc
Summary of 6 Dakin oxidations & journal references.
Di-Br-me.doc
Methylene Bromide; W. Rt. Hartman & E. E. Dreger. (Methane, dibromo-)
Org. Syn. Coll. vol. 1 p357-360.
DMT-Ext.doc
Extracting DMT from Acacia maidenii - net; anon.
Drug-bib.doc
Drug Bibliography: A-S; by
ecst-Faq.doc
Ecstasy FAQ - not yet organized; contains Shulgin's bibliography. Anon; 19 Jun 91
Elec-ox.doc
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Electrolytic Oxidation of Isoeucenol to vanillin; Alexander Lowy & Catherine M. Moore; American Electro-Chemical Society Transactions 1922, vol. 42, p273; (P) LG 30-E(
Elect-red.doc
Preparation of Hydrocinnamic Acid by electrolytic reduction; Ingersoll. Org. Syn. 9, 42, (1929); A. W. Ingersoll; Org. Syn. Coll. vol. 1, p 311-314.
Elks-43.doc
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?-3:4-Methylenedioxy-phenyl-isopropylamine. By J. ELKS and D. H. HEY. Glycidic ester condensation method.
Epoxidation.doc
Epoxidation and Hydroxylation of Ethylenic Compounds with Organic Peracids - Chapter 7 - by
Daniel Swern.
An improved procedure for the KMnO4 oxidation of olefins to cis-1,2-glycols by use of phase transfer catalysis, William P. Weber and James Peter Shepherd. Tetrahedron Letters No. 48, pp 4907 - 4908, 1972.
Eugenol.doc
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1. Eugenol and Isoeugenol; S Arctander, Perfume & Flavour Chemicals, Arctander, NY, 1969, pp 167-172
2. The major components of Indonesian clove leaf oil and Madagascan clove bud oil - Perfumer & Flavorist 20(5), Sept./Oct. 1995, p102
3. Composition of Dill Oil, Perfumer & Flavorist, 21(3), 64 (1996)
Extractr.doc
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The EXXTRACTOR ; Psychedelic Illuminations #6, 88-89.- Extracting substances found in plants.
Fester.doc
Chapters 1 to 5.
Chemicals and Equipment
Preparation of Phenylacetone
Preparation of N-Methylformamide
Leuckart reaction
Crystal formation
Grignard.doc
Morris Kharasch; Reinmuth, Grignard Reactions of Nonmetallic Substances, p 1204-1227; Prentice-Hall, 1954. (B) JU 65-G(15). Aldimines.
Reactions of organomagnesium compounds with aliphatic azomethines and with hexamethylenetetramine. I. Vera Evdokimoff; Gazz. Chim. ital. 77, 318-326 (1947) CA 42:2586c (1948)
Haloalkylation.doc
Haloalkylations, p 659 - from "Friedel-Crafts and Related Reactions vol. 2", 1964, Chp. XXI; George A. Olah & William S. Tolgyesi - Chloromethylation etc.
Harmala_ext.txt
Extraction of alkaloids from Peganum harmala. From "The Alkaloids" Vol. II by Manske (p393).
HBr.txt
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H. E. Carter, Metabolism of Amino Acids, J. Biol. Chem. 108, 1935, p 623. HBr addition to alkene with Eleusis discussion.
Hofmann.doc
1. A Re-examination of Limitations of the Hofmann Reaction; December 1958, p 2029; Magnien & Baltzly
2. The Hofmann Reaction; Wallis & Lane; Organic Reactions Vol. 3, p268, 1947
Hydrazine doc
Prep. Hydrazine Sulfate from ammonia and sodium hypochlorite; Adams and Brown. Org. Syn. 2, 37 (1922);
Org. Syn. Coll. Vol. 1 2nd ed., 309 (1941)
Ide&Buck.doc
4-Aminoveratrole (3,4-dimethoxy-Aniline). J. S. Buck and W. S. Ide. Amide + bleach --> Amine.
Illicium Parviflorum.doc
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Journal of the American Pharmaceutical Association vol. 27, pp 573-4, July 1938. "A Note on the Volatile Oil of Illicium Parviflorum Michx". By P. A. Foote. Contains > 90% Safrole
Imine-reduction.doc
The Chemistry of the Carbon-Nitrogen Double Bond, page 506: Electrochemistry of the Carbon-Nitrogen Double Bond - In "The Chemistry of the functional groups" Interscience, 1970, ed Patai. (B) K 20, s131516000
Henning Lund - Electrolytic reduction of imines to amines.
Indan.doc
5,6-(methylenedioxy)-2-aminoindan HCl - Nichols et al, J. Med Chem. 1990, 33, 703.