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Does not work, extremely low yield.
im really not sure how to explain but how about using sodium sulfite? p2p not the oxime tho
Quote from: Hanswurst on July 24, 2016, 09:55:08 AMDoes not work, extremely low yield.Thanks for reporting Hans!can you go a bit into detail I assume you reduced some nitropropene to the alleged oxime followed by Mg reduction?Did you isolate it in between?
Quote from: b6baddawg on July 24, 2016, 03:49:48 PMim really not sure how to explain but how about using sodium sulfite? p2p not the oxime thoWhy in the earth one would want to get rid of the nitrogen which has been placed there in the first hand?