2 grams Oxime was put together with 75 ml meoh and a huge amount of Nabh4 (0,75 grams). Great bubble evolution.
Hcl was added to maintain the ph 7-8.
After 1 hour the mixtur was processed ala Shulgin.
0,6 grams suspect pmoh freebase was solid in isopropanol and soluble in water also that is sure not the oxime.
Freebase was dissolved in DCM.
Isopropanol was saturated wit Citric acid, added to DCM.
DCM was evaporated in waterbad with vigorous stirring . A white precipitate was in the bottom of the flask.Propanol was poured of.
The white precipitate was rinsed with a small amount of water and recristallized from dH2O to give 0,5 grams white orange needles. Bioessay of this citrate will happen today evening 75 mg.