Author Topic: ethylamine  (Read 1296 times)

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Rhodium

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Check out Vogel's book at my page too.
« Reply #20 on: November 28, 2002, 11:35:00 AM »
Check out Vogel's book at my page too.

pickle11

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ethyl iodode and ammonia
« Reply #21 on: November 30, 2002, 09:36:00 AM »
the comlete book of ecstacy
chapter 9
LSD synth

https://www.thevespiary.org/rhodium/Rhodium/chemistry/tcboe/chapter9.html



"the other syntheses is diethylamine. It too makes you a marked man. Clandestine chemistry to the rescue. Diethylamine is a side product in the synthesis of ethylamine from ammonia and ethyl iodide which can be maximized with with a mole ratio of 1 to 2 respectively. It can be freed from the other two hydrochlorides (ethylamine, bp 16°C and triethylamine, bp 89°C) by basifying with excess 25% NaOH followed by fractional distillation (diethylamine, bp 55.5°C). "