Author Topic: rxtalization of 2-(chloroacetamido)-5-chlorobenzop  (Read 1390 times)

0 Members and 1 Guest are viewing this topic.

starlight

  • Guest
rxtalization of 2-(chloroacetamido)-5-chlorobenzop
« on: September 17, 2004, 03:06:00 PM »
Hi there,

anyone know what an appropriate rextalization solvent for 2-(chloroacetamido)-5-chlorobenzophenone might be?

many thanks.

java

  • Guest
About your material in question....
« Reply #1 on: September 18, 2004, 11:29:00 PM »
Maybe by checking out this article , you can find your answer.......java

One-Pot Synthesis of 2-(N-Methyl-2-chloroacetamido)-5-chlorobenzophenone

CHINESE JOURNAL OF PHARMACEUTICALS, 26, 49,1995


it may be archived here.....

http://zgyygy.periodicals.net.cn/default.html



I found the reference here using a korean search engine.....

http://science.empas.com/search/kisti_detail.html?sn=20051743033




Rhodium

  • Guest
Lit. mp.
« Reply #2 on: September 19, 2004, 03:02:00 AM »
Melting Points (with recrystallization solvent and Literature reference) for CAS [4016-85-7]

119-121°C   (ethanol) J.Org.Chem. 27, 562 (1962)
117-118°C   (benzene, petroleum ether) J.Org.Chem. 27, 3781 (1962)
117-118°C   (benzene, diethyl ether, petroleum ether)

Patent DE1136709

(Chem.Abstr. 59, 12827, 1963)