Author Topic: Mescaline extraction question  (Read 712 times)

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a3d0a3m

  • Guest
Mescaline extraction question
« on: November 01, 2003, 06:43:00 AM »
I am planning a extraction ala

https://www.thevespiary.org/rhodium/Rhodium/chemistry/mescaline.extraction.html

and I have a question. After basifying and extracting mescaline freebase w/ non-polar, is it possible to avoid adding dilute acid to the non-polar and instead just gassing with Cl2 to salt the mescaline out of the n-p?

Bandil

  • Guest
Dont add Cl 2 , that would be *DUMB*!
« Reply #1 on: November 01, 2003, 10:50:00 AM »
Dont add Cl2, that would be *DUMB*! You could add HCl though  8) .

Anyhow, i think that the mescaline is to impure to crystallize just like that. So i'd definately chose the route their using in that document!


a3d0a3m

  • Guest
Oops
« Reply #2 on: November 01, 2003, 08:26:00 PM »
My revised plan I guess is to add dilute sulfuric acid to the np/freebase and then recrystalize the mescaline sulfate with hot distilled water. My question now is what pH should I be aiming for in the aqueous layer?