Author Topic: intersting article on mdma synthesis circa 2010  (Read 203 times)

jon

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intersting article on mdma synthesis circa 2010
« on: May 29, 2011, 06:37:10 AM »
enjoy, many AMBP related methods and references

Evilblaze

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Re: intersting article on mdma synthesis circa 2010
« Reply #1 on: May 29, 2011, 12:13:49 PM »
There is a little mispelling in the article.

The compound named "h*******" is piperonal and compound number 10 is the h*****/floramelon.
« Last Edit: November 12, 2011, 05:18:06 PM by Enkidu »

Shake

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Re: intersting article on mdma synthesis circa 2010
« Reply #2 on: May 29, 2011, 01:54:45 PM »
my god.. so it is, well spotted Evil Blaze and shame on you jon for not seeing that it says xxxxx and it looks nothing like it.. jeez who writes these refs
« Last Edit: July 19, 2011, 12:39:14 AM by Enkidu »

jon

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Re: intersting article on mdma synthesis circa 2010
« Reply #3 on: May 29, 2011, 02:30:58 PM »
yeah i noticed that too it did'nt occur to me to mention it well written though.
and paid for by the government thanks guys!
« Last Edit: May 29, 2011, 02:34:58 PM by jon »

Bardo

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Re: intersting article on mdma synthesis circa 2010
« Reply #4 on: May 29, 2011, 09:02:31 PM »
What is compound 17 for the mescaline starting material?.... And the ONLINE publication date is 2010 but I believe the original publication date is 2005.
« Last Edit: May 29, 2011, 09:12:13 PM by Bardo »

Evilblaze

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Re: intersting article on mdma synthesis circa 2010
« Reply #5 on: May 30, 2011, 01:04:18 PM »
Compound 17 is 3,4,5-Trimethoxyphenylpropionic acid, CAS: 25173-72-2.

It is not an easily obtainable precusor.

hypnos

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Re: intersting article on mdma synthesis circa 2010
« Reply #6 on: May 30, 2011, 02:41:02 PM »
  "
-=[Mescaline]=-
4) Gallic acid trimethyl ether + beta-Alanine = Mescaline
5) 3,4,5-trimethoxyphenylacetic acid + glycine = Mescaline
6) 3,4,5-trimethoxyphenylpropionic acid + carbamate = Mescaline

 stolen with thanx --refs if neccessary--refers to 'Kolbe reaction' to effect synth

  Goodnight Hyppy
"the two things you can give away and never lose, are what you know, and how you feel...."

Tsathoggua

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Re: intersting article on mdma synthesis circa 2010
« Reply #7 on: May 30, 2011, 02:51:34 PM »
For no.5, one could also go through the P2P, via destructive distillation of the lead or Ca salts, could they not? although yields may not be as good, likely not. Or is that reaction not compatible with aryl alkoxy substituents present?
Nomen mihi Legio est, quia multi sumus

I'm hyperbolic, hypergolic, viral, chiral. So motherfucking twisted my laevo is on the right side.

hypnos

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Re: intersting article on mdma synthesis circa 2010
« Reply #8 on: May 31, 2011, 09:07:02 AM »
  "For no.5, one could also go through the P2P, via destructive distillation of the lead or Ca salts, could they not? although yields may not be as good"

 Sorr Tsog, me 'mad Matey',, I,, couldnt say,,however, in a few hours, upon my return I shall post the link to that data,, Its pretty interesting but most of it would be, "out of my league" ,,so I'll just give these "good sodoku's" to the 'faster processors' around here, running ALL SORTS of "wetware" as you so beautifully put it--but seems 'Do able'......And I'm getting an idea of just "how neat/nifty/unique and inspirational" the Collective 'wetware' around here is Just as you say......
  "my name is legion, and we are many"...nice!
 Hyppy
"the two things you can give away and never lose, are what you know, and how you feel...."

Tsathoggua

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Re: intersting article on mdma synthesis circa 2010
« Reply #9 on: May 31, 2011, 05:05:26 PM »
Mad? I will have you know I am perfectly sane, thank you.

Although my definition of the word might not be the same as other peoples.
Nomen mihi Legio est, quia multi sumus

I'm hyperbolic, hypergolic, viral, chiral. So motherfucking twisted my laevo is on the right side.

hypnos

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Re: intersting article on mdma synthesis circa 2010
« Reply #10 on: June 01, 2011, 01:49:28 AM »
   Lol
"the two things you can give away and never lose, are what you know, and how you feel...."

meme

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Re: intersting article on mdma synthesis circa 2010
« Reply #11 on: December 24, 2012, 03:37:25 PM »
Thanks, jon for the post, and thanks to everyone else for the comments.  Now, to let this lay dead :)