Author Topic: technique for the generation of mdma II citrate  (Read 318 times)

jon

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technique for the generation of mdma II citrate
« on: January 25, 2010, 11:22:29 AM »
conventional means of recrystallizing mdma citrates using ipa acetone fail due to it's solubility in acetone .
a more workable solution has been attained
ctric acid food grade is usually anhydrous having a f.w of 196.4 for every g/mole of mdma base add 1/2 mole of citric acid dissolve in ipa use excess citric acid.
the ip will dissolve the mdma citrate and leave the unreate citric acid undissolved the mdma salt can then be rinsed of the acid with a little ipa (anhydrous)
reduce the volume of the ipa by evaporation and mdma citrate will crstalize from this alone this provides a convenient procedure for preparing mdma citrate.
one caveat the hyrates seem to interfere with crystalization make sure your base is free of water and the alcohol is dry too.
i can't seem to get complete crops and have to resort to rpeated crystallizations ether did'nt help either I think hydrates are the culprit it's tricky.
« Last Edit: January 25, 2010, 04:29:49 PM by jon »

jon

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Re: technique for the generation of mdma II citrate
« Reply #1 on: January 26, 2010, 03:28:23 AM »
ahh i see what i did wrong the ipa did'nt dissolve the citric acid well enough so i had freebase andd some citrate which crystallized soley from ipa.
i'm going to perfect this crystalliation and share the gold with my fellow bees it's still in progress.
« Last Edit: January 26, 2010, 03:48:35 AM by jon »

Naf1

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Re: technique for the generation of mdma II citrate
« Reply #2 on: January 27, 2010, 02:52:14 AM »
I have had good success with MDA*HCl and ethanol, as long as it is dry it does a really good job. One or two drops of (anyone of these; ethyl acetate, diethyl ether, mek, xylene or acetone) does wonders! I am sure you would have good success also with the citrates if you substitute acetone for xylene.

jon

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Re: technique for the generation of mdma II citrate
« Reply #3 on: January 31, 2010, 09:12:24 AM »
mda is a different ballgame it does'nt for  hydrates as does mdma choch is whay mdma can be a bitch some times.

quetzalcoatl

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Re: technique for the generation of mdma II citrate
« Reply #4 on: February 23, 2010, 08:58:10 PM »
so could you prepare some mdma citrate from your mdma freebase, to aid in oral absorption?
that's a backhanded way of saying to the noobs -> make your mdma into mdma citrate for increased potency.