Bisulfite Adduct on Aldehydes.

anime · Sun Aug 28, 2005 11:04 pm

Swim is wanting to prepare a certain 4-ethyl-2,5-dimethoxybenzaldehyde, swim is wondering how he would go about forming the bisulfate adduct to purity for the produce and then release the amine from the complex.

Does the proceedure for forming a ketone bisulfite complex apply to this or is a different approach taken?

Thx.
amine.

joe_aldehyde · huxleys associate

if you had read my earlier post, you would know Wink

UTFSE! stirr your aldehyde with a saturated solution of NaS2O5.

java · Consumer

Here is the thread where the discussion took place ..........java

https://synthetikal.com/synthforum/viewtopic.php?p=9325&highlight=bisulfite+adducts#9325