Pages: 1

Author Topic: Can anyone read a few NMR results for me?  (Read 90 times)

DynoMiTe

  • Larvae
  • *
  • Posts: 3
Can anyone read a few NMR results for me?
« on: April 29, 2012, 07:32:18 PM »
I recently got a few results back from the lab. I however can not read NMR results. The person who usually doe this for me is not available.

This is what the lab wrote along with the results and all four are within one PDF. I am going to try and upload the PDF which is password protected here but if it doesn't upload I will upload it using some hosting website. http://www.pdfhost.net/index.php?Action=Download&File=ea91c1835bf297450a895704bbdf0a8f The password is: 1q47iwrt7
This is the description of each one.
A2012.0001 is AH7921
B2012.0001 is 2cB-fly.
M2012.0005 is 4-meo-pcp hcl
D2012.0001 is desoxypipradrol

Thanks so much!

dream0n

  • Subordinate Wasp
  • ***
  • Posts: 204
Re: Can anyone read a few NMR results for me?
« Reply #1 on: April 29, 2012, 09:16:02 PM »
No, but I can accurately tell you purity could be improved on.
[EDIT]  Do you know if the others ( not 4-meo-pcp as it is indicated) were hcl salts as well, or as the base?
« Last Edit: April 29, 2012, 09:57:29 PM by dream0n »
off to bigger and better things - don't worry I will visit from time to time

lugh

  • Global Moderator
  • Foundress Queen
  • *****
  • Posts: 876
Re: Can anyone read a few NMR results for me?
« Reply #2 on: April 29, 2012, 11:18:14 PM »
Quote
Can anyone read a few NMR results for me?

Not now, but there are a lot of textbooks in digital format that you can use to learn how to do it yourself  ;)  Structure Elucidation by NMR in Organic Chemistry: A Practical Guide by Eberhard Breitmaier has been uploaded to:

https://the-collective.ws/forum/index.php?topic=148.msg161208#msg161208

 8)

Chemistry is our Covalent Bond

Quantum Dude

  • Subordinate Wasp
  • ***
  • Posts: 192
Re: Can anyone read a few NMR results for me?
« Reply #3 on: April 30, 2012, 03:45:33 AM »
You could at least provide us with easily accessible files. That is the least you could do if you want people to help you, Ive tried the password you provided and I am unable to open any of them.

dream0n

  • Subordinate Wasp
  • ***
  • Posts: 204
Re: Can anyone read a few NMR results for me?
« Reply #4 on: April 30, 2012, 06:43:36 AM »
The PDF files attached opened fine for me...
hint the password was removed
« Last Edit: April 30, 2012, 07:00:45 AM by dream0n »
off to bigger and better things - don't worry I will visit from time to time

fractal

  • Subordinate Wasp
  • ***
  • Posts: 110
Re: Can anyone read a few NMR results for me?
« Reply #5 on: April 30, 2012, 12:45:51 PM »
Everything appears to be in order I only checked the number of different proton systems and chemical shifts to compare though. Someone else can check spin splitting, integrated ratios, ect lol
« Last Edit: April 30, 2012, 02:57:30 PM by fractal »
Pages: 1