Author Topic: wacker benzo  (Read 70 times)

mdhard

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wacker benzo
« on: October 09, 2012, 05:21:09 AM »
hi,

I could make a benzo wacker with dmf with 1kg or more of safrole?
I googled but do not see on a larger scale ..

the process could lower incomes? or, the reaction can be scaled without problems?

DMF = 700mL
Water = 100mL
p-benzoquinone = 216g (2M)
PdCl2 = 3.6g
Safrole = 320g

This reaction 3 or 4 times larger, would have a problem?

thanks for any help


Thanks
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fractal

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Re: wacker benzo
« Reply #1 on: October 09, 2012, 12:40:11 PM »
It can be scaled fine, there are threads about it here. Use the search engine ;)