Seeking opinions on fractional columns and condensers to vacuum distill oil of sassafras albidum.
The lengths are all 250mm - 500mm.
Vacuum jacketed fractionating column:
Jacketed fractionating column with tip for vacuum:
Horizontal condenser for fractional distillation of safrole:
These vertical condensers are for reflux and hard to distill stuff.
Condenser for reflux (Al/Hg):
Allihn condenser for reflux (Al/Hg):
Coldfinger with coil for reflux (Al/Hg):
Distillation and reaction vessel will be a 2L - 3L 3-neck RBF.
Safrole distillation apparatus will have a RBF in an oil bath with magnetic stirrer and fractionating column connected via 3-way adapter to the condenser which drains to a 1L RBF via 2-way adapter.
The sourced Xylene and Nitromethane needs to be distilled too and there is hope that 3 pieces of condenser and column glassware will suffice for all of these.
I like the vacuum jacketed fractionating column (not the one with the tip for vacuum) and the coldfinger coil condenser for reflux.
Vacuum for safrole distillation will be applied at the 2-way adapter between the condenser and distillate RBF.
If you had to get only 3 pieces of glassware from those on top, which would it be?
Suggestions for a horizontal condenser for fractional distillation of safrole are welcome.
The lengths are all 250mm - 500mm.
Vacuum jacketed fractionating column:
Jacketed fractionating column with tip for vacuum:
Horizontal condenser for fractional distillation of safrole:
These vertical condensers are for reflux and hard to distill stuff.
Condenser for reflux (Al/Hg):
Allihn condenser for reflux (Al/Hg):
Coldfinger with coil for reflux (Al/Hg):
Distillation and reaction vessel will be a 2L - 3L 3-neck RBF.
Safrole distillation apparatus will have a RBF in an oil bath with magnetic stirrer and fractionating column connected via 3-way adapter to the condenser which drains to a 1L RBF via 2-way adapter.
The sourced Xylene and Nitromethane needs to be distilled too and there is hope that 3 pieces of condenser and column glassware will suffice for all of these.
I like the vacuum jacketed fractionating column (not the one with the tip for vacuum) and the coldfinger coil condenser for reflux.
Vacuum for safrole distillation will be applied at the 2-way adapter between the condenser and distillate RBF.
If you had to get only 3 pieces of glassware from those on top, which would it be?
Suggestions for a horizontal condenser for fractional distillation of safrole are welcome.