Just something i knocked together for steam distilling post al/hg rxn solution.
I used a empty 5litre acetic acid drum as the main distillation vessal.
In the lid i cut a hole and inserted a 24/40 fitting off some broken glassware. pulled it tight and teflon taped it up.
I heated a piece of pyrex - the straight tube section from inside a broken longer spiral coolcoil and pushed that through the top of the drum (i have some cheapo right angle pyrex pieces what would do the job nicely too) its attached to a hose leading to a steam stripper as external steam source.
Put a plate or something similar in bottom of a stew pan,(stops the plastic overheating on the base) the drum inside that, fill pan with water and set it up ready to go..
i fill the drum about 2/3rds full with already pretty warm post reaction solution.(3litre) give it 10-15 minutes to get a bit hotter, adjust the condensor again cos the plastic swells and warps a bit.
Then just let the fucker rip with the external steam source.
once its too temp turn off the gas - yeah its on the cooker lol - the stewpan water insulates enough to let the steam do the work well enough.
The drum rinses clean after distillation - just like that.
Its just an easy alternative if you break your bigass glassware, or get sick of pissing about cleaning it out.
I used a empty 5litre acetic acid drum as the main distillation vessal.
In the lid i cut a hole and inserted a 24/40 fitting off some broken glassware. pulled it tight and teflon taped it up.
I heated a piece of pyrex - the straight tube section from inside a broken longer spiral coolcoil and pushed that through the top of the drum (i have some cheapo right angle pyrex pieces what would do the job nicely too) its attached to a hose leading to a steam stripper as external steam source.
Put a plate or something similar in bottom of a stew pan,(stops the plastic overheating on the base) the drum inside that, fill pan with water and set it up ready to go..
i fill the drum about 2/3rds full with already pretty warm post reaction solution.(3litre) give it 10-15 minutes to get a bit hotter, adjust the condensor again cos the plastic swells and warps a bit.
Then just let the fucker rip with the external steam source.
once its too temp turn off the gas - yeah its on the cooker lol - the stewpan water insulates enough to let the steam do the work well enough.
The drum rinses clean after distillation - just like that.
Its just an easy alternative if you break your bigass glassware, or get sick of pissing about cleaning it out.