swip see this article in org syn, and vogel 3ed and if wonder that reaction work up with chloroephedrine , any idea is welcome
Reduction via grignard
« on: September 13, 2009, 10:51:48 PM »
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Topic: Reduction via grignard (Read 85 times)
POSEIDON
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n-hexane.pdfSedit
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Re: Reduction via grignard
« Reply #1 on: September 13, 2009, 11:39:28 PM »
As much as I despies questions such as "here is a procedure I know nothing about can you tell me if it makes meth" I would say yes is should work fine. How do you plan on chlorinating Ephedrine might I ask?
I also must say that if you need to ask then chances are the grignard is a bit out of reach don't ya think? I am no great chemist by far but knowing my limitations is a big part any success I might have had.
I also must say that if you need to ask then chances are the grignard is a bit out of reach don't ya think? I am no great chemist by far but knowing my limitations is a big part any success I might have had.
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Re: Reduction via grignard
« Reply #2 on: September 14, 2009, 03:37:41 AM »
swip thinks you can get Chloroephedrine via Lucas reagent (http://en.wikipedia.org/wiki/Lucas'_reagent), then you turn this in meth via grignard , other way is this :
http://designer-drugs.com/pte/12.162.180.114/dcd/chemistry/meth.impurities2.html
swip know magnesium is hard to find , but not imposible and diethyl eter is not hard to make , only need precaution.
http://designer-drugs.com/pte/12.162.180.114/dcd/chemistry/meth.impurities2.html
swip know magnesium is hard to find , but not imposible and diethyl eter is not hard to make , only need precaution.
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