This one was recently requested at SM. I'd like to get a collection of articles about using a DCM/HNO3 mix to perform nitrations posted here. If anyone wants to upload the old .rar about using DCM to extract nitric acid, feel free. I might post it later today....
A Low Hazard Procedure for the Laboratory Preparation of Polynitrate Esters
MARKEN et al
Synthesis 1977; 1977: 484-485 DOI: 10.1055/s-1977-24454
A Low Hazard Procedure for the Laboratory Preparation of Polynitrate Esters
MARKEN et al
Synthesis 1977; 1977: 484-485 DOI: 10.1055/s-1977-24454
A Low Hazard Procedure for the Laboratory Preparation of Polynitrate Esters.PDF