So this 236ml bottle of aq. KI solution has a pretty impressive potential amount of iodine in it. 'Gauranteed Analysis' on the bottle states
Iodide (min)...................0.0794%
That would be 18.73g of Iodide. Stuff is cheap and I found stacks of such bottles at the first big pet supplies store I walked into.
It lists the ingredients as folllows:
De-ionized water, potassium iodide, sodium hydrogen carbonate(goes by the alias sodium bicarbonate sometimes), sodium carbonate, sodium tetraborate(aka Borax)
I tried both trusted methods for claiming I2 out of similar mixtures, with seperate test trials using every which way possible excess, or miinimum, or fridge cooling, or giving it several hours.
Never more than a slight yellowish color.
A wikipedia article or two has led me to conclude that the purpose of the borax is to 'inhibit precipitation'. It sure works. Any ideas?
Iodide (min)...................0.0794%
That would be 18.73g of Iodide. Stuff is cheap and I found stacks of such bottles at the first big pet supplies store I walked into.
It lists the ingredients as folllows:
De-ionized water, potassium iodide, sodium hydrogen carbonate(goes by the alias sodium bicarbonate sometimes), sodium carbonate, sodium tetraborate(aka Borax)
I tried both trusted methods for claiming I2 out of similar mixtures, with seperate test trials using every which way possible excess, or miinimum, or fridge cooling, or giving it several hours.
Never more than a slight yellowish color.
A wikipedia article or two has led me to conclude that the purpose of the borax is to 'inhibit precipitation'. It sure works. Any ideas?

