Some difficulties to perform it, more to Eugenol that has an OH group at benzene ring prone to dimmerization instead of polymerization cause of the double bond. It should be much easier for non phenol substances like 3-ethoxy-4methoxy allylbenzene, plain allylbenzene, or methylenedioxy....
The addition compound is phenylisopropyl hydrogen sulphate (and derivative), that is an acid, say this compound has been successfully isolated, then neutralized with ammonia --> phenylisopropyl ammonium sulphate, a salt.
I'm wondering what will happen if;
1. bring this phenylisopropyl ammonium sulphate at high temperature, is rearrangement will be occured? or
2. mix this salt with solution of ammonia in MeOH, and reflux.
Is it yielding a primary amine?
Any thought?
If primary amine is the yield, then worth to discuss this thread title, how to perform the H2SO4/H3PO4 addition
The addition compound is phenylisopropyl hydrogen sulphate (and derivative), that is an acid, say this compound has been successfully isolated, then neutralized with ammonia --> phenylisopropyl ammonium sulphate, a salt.
I'm wondering what will happen if;
1. bring this phenylisopropyl ammonium sulphate at high temperature, is rearrangement will be occured? or
2. mix this salt with solution of ammonia in MeOH, and reflux.
Is it yielding a primary amine?
Any thought?
If primary amine is the yield, then worth to discuss this thread title, how to perform the H2SO4/H3PO4 addition