What's the deal with the Vacuum method? Is there a special secret here?
I used Baalchemists writeup. There must be something very very simple here that I still don't understand. 54g hex + 185ml 28% HCL (diluted from 162ml 370g/l 32%) I wish they would write it in grams! not ml. It all dissolved, didn't wait to see hydrolysis, I've used this hex before. Put it straight into a hot water bath and refluxed with vacuum for 3 hours. Liquid temp was 78 deg. Then vacuum distilled for 3 hours untill almost dry. Added 85 ml IPA, boiled for 30 min, decanted, results- maybe 10 flakes of MeHN3.HCL. Jesus.
Summarian, and others at the Hive claimed 80 to 95% refluxing at 65 deg. I believe them, but what's the catch?
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