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emulsion?

Started by chiliuno, January 10, 2003, 03:28:00 PM

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chiliuno

i've been distilling bay leaves to get good at distillation...i'm set up properly, but my distillate is not seperating into distinct layers in the seperatory funnel...instead, i get one big layer of cloudy water with a very strong smell.
what would be the best way to isolate the oil?  i tried salting the mess, but now i just have salt at the bottom of the funnel.
any ideas?


hCiLdOdUeDn

Extract with some DCM or other non-polar solvent and distill off the solvent to leave the oil.


chiliuno

that's what i thought, but hearing it from an experienced chemist and reading it in a textbook are two diff things...thanks for the help!