Author Topic: PCP and Relatives: A Synthetic View  (Read 1698 times)

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Aurelius

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PCP and Relatives: A Synthetic View
« on: May 12, 2004, 09:50:00 PM »
Bear with me, this is a completely new project and I've got hundreds of links to put in.  I'm very busy and this might take a few weeks or longer- but it's a popular enough topic that I thought it would be worth it.

PCPstraight-up

https://www.thevespiary.org/rhodium/Rhodium/chemistry/pcp.shulgin.html


https://www.thevespiary.org/rhodium/Rhodium/chemistry/pcp/cn_synth.html


Post 288137

(Antoncho: "A cool PCP synthesis", Novel Discourse)


Ideas on PCP Synthesis:

Post 475464

(ning: "phencyclidine sans cyclohexanone", Novel Discourse)


Analogues:

PCPy: Pyrrolidene analogue:

Post 101681 (missing)

(The Alchemist: "Dust for the masses...", Chemistry Discourse)
(read the whole thread)

4-MeO-PCP

https://www.thevespiary.org/rhodium/Rhodium/chemistry/4-meo-pcp.html



Fluorinated Analogues:

Post 471106

(Rhodium: "Fluorinated PCP Analogs", Methods Discourse)


Contaminants:

Post 382798

(Rhodium: "PCP byproducts", Methods Discourse)

https://www.thevespiary.org/rhodium/Rhodium/chemistry/pcp.pcc.analysis.html


Post 406851

(Rhodium: "Measuring PCC contamination of PCP", Methods Discourse)
(same as above page)

Post 502110

(Rhodium: "Pyrolytic Fate of the PCP contaminant PCC", Methods Discourse)


TCP

Post 484668

(Xicori: "TCP Synthesis", Methods Discourse)

Bioassays

Post 486907

(Xicori: "Bioassay", Methods Discourse)


Contamination
PCC Detection

https://www.thevespiary.org/rhodium/Rhodium/chemistry/pcp.pcc.analysis.html



PCDE

Synth and Bioassay

Post 369598

(Antoncho: "Zealot: synthesis and bioevaluation of PCDE", Novel Discourse)


PCM

Post 475049

(Xicori: "PCM synthesis", Methods Discourse)

Bioassay

Post 475116

(Xicori: "thanks for the flowers :-D details on bioassay", Methods Discourse)


Ketamine

https://www.thevespiary.org/rhodium/Rhodium/chemistry/ketamine.html


https://www.thevespiary.org/rhodium/Rhodium/chemistry/ketamine2.html



analogues:

Post 465673

(Manichi: "Discussion on possible ketamine analogs", Novel Discourse)

Post 505521

(ning: "Modified ketamine method", Novel Discourse)


Refs:If the refs aren't here in this digest  or elsewhere at the Hive (so do a search), they would be appreciated.

Post 466915

(Manichi: "Ketamine References Feeding", Novel Discourse)

Post 466993

(Rhodium: "Ketamine Reference Feeding #2", Novel Discourse)


Tiletamine (SP?)

Eticylclidine

https://www.thevespiary.org/rhodium/Rhodium/chemistry/eticyclidine.html



Rolicylidine

https://www.thevespiary.org/rhodium/Rhodium/chemistry/eticyclidine.html




Others?

Please feel free to pm links, comments, suggestions etc. to Aurelius on this Digest or any others maintained by me.

MISC TO BE PLACED:

Post 455365

(Bwiti: "Novel Phenylcyclohexylamines..", Methods Discourse)

Post 424992

(Bwiti: "1-(1-Phenylcyclohexyl)-4-phenylpiperidine", Methods Discourse)


Patents:
contributed by Cyrax in:

Post 356567

(Cyrax: "PCP Patents, a compendium", Methods Discourse)

Patent GB836083


Patent GB837747


Patent US2921076


Patent US3097136


Patent US3145229


Patent US5248686




Contributed by Bwiti in:

Post 357544

(Bwiti: "That's good news!", Methods Discourse)

Patent GB758143


Patent GB838748


Patent GB853775


Patent GB861350


Patent US3192219


Patent US3097207

 

Patent GB836083

 

Patent GB837747

 

Patent US5969159

 

Patent US3097136


Patent US3145229


Patent US3097136


Patent US3247200


Patent US3522273


Patent US2921076


Patent US3254124



References Requested Specifically for this Digest:

Post 361229

(Bwiti: "Needed References", Methods Discourse)

(before sending of these refs- be sure that they haven't already been posted here or in posts subsequent to 361229 in that same thread)

Post 361271

(Rhodium: "More PCP", Methods Discourse)

Post 378784

(Rhodium: "Rigid PCP Analogs - Binding to Sigma/PCP receptors", Methods Discourse)


Mostly Pharm info, but some synth:

Post 507205

(7is: "More PCP related studies", Methods Discourse)
-- be sure to check the following threads also.

Precursors
Cyclohexanone
by ox. of Cyclohexanol
with KMnO4

Post 285993

(Elementary: "Oxidation of cyclohexanol with KMnO4", Methods Discourse)


1,5-Dibromopentane:

Post 436097

(pHarmacist: "1,5-dibromopentane", Methods Discourse)

Post 288137

(Antoncho: "A cool PCP synthesis", Novel Discourse)

Post 184706

(Rhodium: "Re: Help to make 1,5-dibromopentane (Method). for PCP", Novel Discourse)


PCA:

Post 105162 (missing)

(Slappy: "Re: PCA question", Chemistry Discourse)



PCC: 1-Piperidinyl Cyclohexanecarbonitrile (& analogues)

Post 172690 (missing)

(slappy: "Re: Weight of PCC-Analogue(from methylamine).....", Chemistry Discourse)

Post 101408 (missing)

(Beagle: "Re: Question about 1-piperidine-carbonitrile...", Chemistry Discourse)


--

Post 465740

(josef_k: "phenylcyclopentylketone", Novel Discourse)

Post 465792

(Manichi: "Cyclohexene -persulfate/CuSO4->CyclopentaneCOOH", Novel Discourse)

Post 466155

(Vitus_Verdegast: "Great work Manichi!!", Novel Discourse)