From my ignorance...and being a newbie here.... but with all times great succes,i usually dissolve the final puffy mdma,totally dried and acetone cleaned on a minimun amount of lab grade boiling methanol,onlly ussing the minumun to total disolve the batch.Then let it cool slowly and let it evaporate at ambiente temperature.It takes like 2-3 days,with almost all the methanol way out on the first day and endding with a beaker plenty of oilly crystals that takes two days more to completly get oil free-dry-crystallized.
That gave me beatifull weird flat cubic crystalls 0,5 cm large ,and on good cases,letting the beaker alonge without curiosity shakings,get all the bottom of the beaker polimerized like candyrock.I think that it´s what you want,and would be the easiest way to get it for the lazy chemist...like me
I make that with small amounts,like 15 gr product,...but supposed to work on so bigger amounts.
Try to understand us about enantyomer issolation...to me...at this moment...seems to be things of the future!