Author Topic: 2011 Reference Requests (Read 3668 times)

Shake · « **Reply #80 on:** May 01, 2011, 02:32:53 PM »

Wacker-Type Oxidation of Internal Olefins Using a PdCl2/N,N-Dimethylacetamide Catalyst System under Copper-Free Reaction Conditions†

1. Takato Mitsudome Dr.1,
2. Keiichi Mizumoto1,
3. Tomoo Mizugaki Dr.1,
4. Koichiro Jitsukawa Prof.?Dr.1,
5. Kiyotomi Kaneda Prof.?Dr.1,2

Article first published online: 28 DEC 2009

DOI: 10.1002/anie.200905184

THIS ONE TOO!

A simple catalyst system consisting of PdCl2 and N,N-dimethylacetamide (DMA) as the solvent can successfully promote Wacker-type oxidation of internal olefins. This catalyst system does not require copper compounds and is tolerant of a wide range of substrates having internal olefins.

xxxxx · « **Reply #81 on:** May 01, 2011, 08:04:12 PM »

No problem no1unom, I created the May referance thread if you would like to sticky it.
Heres that ref again:

Synthesis protocol influence on aqueous magnetic fluid properties
M. Racuciu,
Current Applied Physics, Volume 9, Issue 5, September 2009, Pages 1062-1066
DOI: 10.1016/j.cap.2008.12.003.

And as requested by Shake:

Wacker-Type Oxidation of Internal Olefins Using a PdCl2/N,N-Dimethylacetamide Catalyst System under Copper-Free Reaction Conditions
Mitsudome, T., Mizumoto, K., Mizugaki, T., Jitsukawa, K. and Kaneda, K. (2010),
Angewandte Chemie International Edition, 49: 1238–1240.
doi: 10.1002/anie.200905184

Evilblaze · « **Reply #82 on:** May 02, 2011, 01:45:01 AM »

Sugasawa Indole Synthesis
DOI: 10.1002/9780470638859.conrr611
http://onlinelibrary.wiley.com/doi/10.1002/9780470638859.conrr611/abstract

ChemInform Abstract: Simple One-Step Syntheses of Indole-3-acetonitriles from Indole-3-carboxaldehydes.
F. YAMADA,
DOI: 10.1002/chin.199816110
Volume 29, Issue 16, page no, April 21, 1998
http://onlinelibrary.wiley.com/doi/10.1002/chin.199816110/abstract

Iron(III) Tosylate in the Preparation of Dimethyl and Diethyl Acetals from Ketones and ?-Keto Enol Ethers from Cyclic ?-Diketones
Synthetic Communications: An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, Issue 15, 2008, Pages 2607 - 2618
Authors: Horacio Mansillaa; Mariacutea M. Afonsob
DOI: 10.1080/00397910802219361

The Chemistry of Imines.
Robert W. Layer
Chem. Rev., 1963, 63 (5), pp 489–510
DOI: 10.1021/cr60225a003
http://pubs.acs.org/doi/abs/10.1021/cr60225a003

Substituted Naphthofurans as Hallucinogenic Phenethylamine?Ergoline Hybrid Molecules with Unexpected Muscarinic Antagonist Activity
Aaron P. Monte
J. Med. Chem., 1998, 41 (12), pp 2134–2145
DOI: 10.1021/jm980076u
http://pubs.acs.org/doi/abs/10.1021/jm980076u

ChemInform Abstract: An Application of the Stille Coupling for the Preparation of Arylated Phthalonitriles and Phthalocyanines.
Viviane Aranyos,
DOI: 10.1002/chin.199950094
Volume 30, Issue 50, page no, December 14, 1999
http://onlinelibrary.wiley.com/doi/10.1002/chin.199950094/full

Thanks!

xxxxx · « **Reply #83 on:** May 02, 2011, 03:36:32 PM »

ChemInform Abstract: Simple One-Step Syntheses of Indole-3-acetonitriles from Indole-3-carboxaldehydes.
F. YAMADA,
DOI: 10.1002/chin.199816110
Volume 29, Issue 16, page no, April 21, 1998
http://onlinelibrary.wiley.com/doi/10.1002/chin.199816110/abstract

Iron(III) Tosylate in the Preparation of Dimethyl and Diethyl Acetals from Ketones and B-Keto Enol Ethers from Cyclic B-Diketones
Horacio Mansillaa; Mariacutea M. Afonsob
Synthetic Communications: An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, Issue 15, 2008, Pages 2607 - 2618
DOI: 10.1080/00397910802219361

The Chemistry of Imines.
Robert W. Layer
Chem. Rev., 1963, 63 (5), pp 489–510
DOI: 10.1021/cr60225a003
http://pubs.acs.org/doi/abs/10.1021/cr60225a003

Substituted Naphthofurans as Hallucinogenic Phenethylamine?Ergoline Hybrid Molecules with Unexpected Muscarinic Antagonist Activity
Aaron P. Monte
J. Med. Chem., 1998, 41 (12), pp 2134–2145
DOI: 10.1021/jm980076u
http://pubs.acs.org/doi/abs/10.1021/jm980076u

ChemInform Abstract: An Application of the Stille Coupling for the Preparation of Arylated Phthalonitriles and Phthalocyanines.
Viviane Aranyos
DOI: 10.1002/chin.199950094
Volume 30, Issue 50, page no, December 14, 1999
http://onlinelibrary.wiley.com/doi/10.1002/chin.199950094/full

Sorry the first ref wasen't available to me. Hope these help you. Looking up references sure beats studying

Bluebottle · « **Reply #84 on:** May 04, 2011, 03:27:08 PM »

Structure-Activity Relationships at Human and Rat A2B Adenosine Receptors
of Xanthine Derivatives Substituted at the 1-, 3-, 7-, and 8-Positions
Soon-Ai Kim,† Melissa A. Marshall,‡ Neli Melman,† Hak Sung Kim,† Christa E. Mu¨ ller,§ Joel Linden,‡ and
Kenneth A. Jacobson
J. Med. Chem. 2002, 45, 2131-2138

xxxxx · « **Reply #85 on:** May 04, 2011, 08:14:04 PM »

Palladium-Catalyzed Oxidation of Phenyl-Substituted Alkenes using Molecular Oxygen as the Sole Oxidant
Bueno, A., de Souza, Á. and Gusevskaya, E. (2009),
Advanced Synthesis & Catalysis, 351: 2491–2495.
doi: 10.1002/adsc.200900294

Hope that helps, sorry couldn't get the other one yet! Wow this is a lot of really new useful research! Dimetylacetimide looks so useful, if only it was OTC, well a bee can dream can't he!

Bluebottle · « **Reply #86 on:** May 04, 2011, 08:36:32 PM »

Palladium-Catalyzed Aerobic Oxidation of Naturally Occurring Allylbenzenes as a Route to Valuable Fragrance and Pharmaceutical Compounds
Luciana A. Parreira, Luciano Menini, Joyce C. da Cruz Santos, Elena V. Gusevskaya
DOI: 10.1002/adsc.201000050

You're welcome Shake and OoBYCoO

Bluebottle · « **Reply #87 on:** May 05, 2011, 02:33:05 PM »

Palladium-Catalyzed Oxidation Reactions: Comparison of Benzoquinone and Molecular Oxygen as Stoichiometric Oxidants
Organometallic Oxidation Catalysis
Topics in Organometallic Chemistry, 2007, Volume 22/2007, 149-189,
DOI: 10.1007/3418_039

Quote

Ps Roid rage this ones for you!

Sedit · « **Reply #88 on:** May 05, 2011, 03:20:54 PM »

Potassium Hydroxide Catalyzed Addition of Arylamines to Styrenes
Daniel Jaspers, Sven Doye
DOI: 10.1055/s-0030-1260555 7 February 2011

Abstract
Potassium hydroxide is a competent and cheap catalyst for the intermolecular addition of arylamines to styrenes. The reactions are performed in nontoxic dimethyl sulfoxide and can be used for the large-scale synthesis of ?-phenylethylamines.

Key words
alkenes - amines - styrenes - potassium hydroxide - base-catalyzed hydroamination - ?-phenylethylamines

https://www.thieme-connect.com/ejournals/abstract/synlett/doi/10.1055/s-0030-1260555

>>DOWNLOAD<<

Sedit · « **Reply #89 on:** May 06, 2011, 03:50:42 AM »

I have never desperately needed a reference this much in my life please help if you can.

Russian Journal of Electrochemistry
Volume 37, Number 9, 893-898, DOI: 10.1023/A:1011936024454

Strategy for Controlling the Kolbe Electrosynthesis in the Presence of Aromatic Fragments and Amino Groups in the Molecule

Abstract
A general characteristic of processes that occur during anodic oxidation of phenylacetic and phenylpropionic acids and derivatives of - and -amino acids on platinum electrodes in methanol and mixed pyridine–methanol solutions is given. From preparative electrolyses in stagnant and flow-through reactors, conditions are determined under which the dimerization (Kolbe electrosynthesis) is least complicated by the formation of polymer products. Properties of removed electrodes, on which stable polymer films formed during the electrosynthesis, are examined. For films formed in certain conditions on the cathode, the presence of a quasi-reversible redox transition is demonstrated. Such films contain disperse platinum codeposited with polymer as a result of the anode dissolution in the cells with common compartments. In principle, the film-modified electrodes can be used for controlling anodic decarboxylation.

Abstract link:http://www.springerlink.com/content/p2t3803161483w60/

Quote from: Sedit on May 06, 2011, 03:50:42 AM

I have never desperately needed a reference this much in my life please help if you can.

OMG SEDIT.. QUIT TRYING TO SUCK MY DICK!
You Said if you do me this favor I have to do something for you sheeshh.... some people are just ungreatful

xxxxx · « **Reply #90 on:** May 06, 2011, 01:18:29 PM »

Preparation and Properties of an Aqueous Ferrofluid
Patricia Berger, Nicholas B. Adelman, Katie J. Beckman, Dean J. Campbell, Arthur B. Ellis, George C. Lisensky
J. Chem. Educ., 1999, 76 (7), p 943
DOI: 10.1021/ed076p943

xxxxx · « **Reply #91 on:** May 08, 2011, 08:09:46 PM »

Dimethyldioxirane oxidation of primary amines
Jack K. Crandall, Thierry Reix
J. Org. Chem., 1992, 57 (25), pp 6759–6764
DOI: 10.1021/jo00051a017

xxxxx · « **Reply #92 on:** May 08, 2011, 09:57:12 PM »

Anodic Decarboxylation of Carboxylic Acids
James A. Waters
J. Org. Chem., 1964, 29 (2), pp 428–430
DOI: 10.1021/jo01025a044

Shake · « **Reply #93 on:** May 09, 2011, 12:31:55 AM »

The Wacker Reaction and Related Alkene Oxidation Reactions
Takacs J.M.; Jiang X-t.
Current Organic Chemistry, Volume 7, Number 4, March 2003 , pp. 369-396(28) DOI: 10.2174/1385272033372851

Quote

The objective of this review is to survey the current state of the Wacker and related alkene oxidation reactions focusing on the reactions of higher alkenes and emphasizing the mechanistic pictures that have evolved, the current understanding regarding issues of selectivity, recent applications of the chemistry in synthesis, and the use of other transition metal catalysts to effect related oxidation reactions.

Shake · « **Reply #94 on:** May 09, 2011, 11:57:59 PM »

Alkylation of Para Quinones with Acyl Peroxides
First PageHi-Res PDF[667 KB]Louis F. Fieser, Albert E. Oxford
J. Am. Chem. Soc., 1942, 64 (9), pp 2060–2065
DOI: 10.1021/ja01261a015

there you go boss

Bluebottle · « **Reply #95 on:** May 10, 2011, 03:10:28 AM »

Heat of Formation of Propylene Oxide

Sinke,G;Hildenbrand,D
J. Chem. Eng. Data.
Vol.7(1) 1962 p.74
DOI: 10.1021/je60012a022

No Abstract

Shake · « **Reply #96 on:** May 10, 2011, 03:22:34 AM »

CXXIV.—The oxidising properties of sulphur dioxide. Part I. Iron chlorides
William Wardlaw and Francis Herbert Clews
J. Chem. Soc.(Trans) Vol.117 (1920) 1093-1103
DOI: 10.1039/CT9201701093

Bluebottle · « **Reply #97 on:** May 10, 2011, 04:01:43 PM »

Quote from: no1uno on May 10, 2011, 08:56:51 AM

An Improved Preparation of Gentisic Acid

Lowenthal,Julius;Pepper,J
J. Am. Chem. Soc
Vol.72(7) (1950) pp.3292–3293
DOI: 10.1021/ja01163a521

No Abstract

Formation of 2,5-dihydroxybenzoic acid during the reaction between singlet oxygen (1O2) and salicylic acid: analysis by ESR oximetry and HPLC with electrochemical detection[/u][/b]

Kalyanaraman,B;Ramanujam,Sujatha;Singh,Ravinder;Joseph,Joy;Feix,Jimmy

J. Am. Chem. Soc
Vol.115(10) (1993) pp.4007–4012
DOI: 10.1021/ja00063a021

No Abstract

Oxidations with potassium nitrosodisulfonate (Fremy's radical). Teuber reaction.

Zimmer,Hans;Lankin,David;Horgan,Stephen

Chem. Rev.
Vol.71(2) (1971) pp.229-246
DOI: 10.1021/cr60270a005

No Abstract

Undergraduate experiments with a long-lived radical (Fremy's salt): Synthesis of 1,4-benzoquinones by degradative oxidation of p-hydroxybenzyl alcohols

Morey,J

J.Chem.Ed.
Vol.65(7) (1988) p.627-
DOI: 10.1021/ed065p627

Abstract

The long-lived, stable radical described in this article can be prepared and stored for several months and therefore is an excellent basis for a series of experiments that the author designed for his class.

Polar additions to olefins and acetylenes. VI. Nonstereospecific addition of bromine to 1-phenylpropene and trans-anethole

Fahey,Robert;Schneider,Hans
J. Am. Chem. Soc
Vol.90(16) (1968) pp.4429-4434
DOI: 10.1021/ja01018a040

Abstract

It has been established that addition of bromine to cis- and trans-1-phenylpropenes and to trans-anethole in carbon tetrachloride occurs by an electrophilic mechanism and that the additions are non-stereospecific. Bromine addition to cis-1-phenylpropene gives a mixture of erythro- and threo-(1,2-dibromopropyl]benzenes in which the ratio erythro:threo is 17:83 and addition to trans-1-phenylpropene yields a mixture of the same dibromides in which the erythro:threo ratio is 88:12. Bromine addition to trans-anethole yields erythro- and threo-p-(1,2-dibromo-propyl)anisoles with an erythro:threo ratio of 63:37, a value quite close to the equilibrium ratio of 67:33. In all cases it was shown that the starting olefins and the product dibromides are stable to the reaction conditions. Relative rates, determined by the competition method, were found to be: styrene, 1.00; cis-1-phenylpropene, 2.1 +/- 0.2; trans-1-phenylpropene, 4.0 +/- 0.5; trans-anethole, 1000 +/- 200. The results are taken as evidence that the intermediate cation formed in the reactions resembles an open benzylic cation more than a bromonium ion.

Bluebottle · « **Reply #98 on:** May 10, 2011, 04:10:11 PM »

Quote from: no1uno on May 10, 2011, 12:51:54 PM

Breaking it up a little

Electrophilic Aromatic Bromination Using Bromodimethylsulfonium Bromide Generated in Situ

Majetich,George;Hicks,Rodgers;Reister,Steven

J.Org.Chem.
Vol.62(13) 1997 pp.4321-4326
DOI: 10.1021/jo970135w

Abstract

It has been shown that bromodimethylsulfonium bromide, generated in situ by treating dimethyl sulfoxide with aqueous hydrobromic acid, is a milder and more selective reagent for electrophilic aromatic bromination than elemental bromine.

Synthetic Routes to 3,4,5-trimethoxybenzaldehyde (Review)

Erofeev,Yu;Afanas'eva,V;Glushkov,R

Pharm. Chem. Journal
Vol.24(7) (1990) pp.501-510
DOI: 10.1007/BF00765001

Abstract

3,4,5-Trimethoxybenzaldehyde (I) is a key intermediate in the synthesis of trimethoprim[2,4-diamino-5-(3,4,5-trimethoxybenzyl)pyrimidine], which, in addition to its antibacterial activity [9], possesses the property of significantly strengthening the bacteriacidal activity of sulfanilamide preparations; it is widely used with the latter in medical practice [9, 47]

Synthesis of Syringaldehyde

Pearl,Irwin

J.Am.Chem.Soc
Vol.70(5) 1948 pp.1746-1748
DOI: 10.1021/ja01185a020

No Abstract

Reactions of Vanillin and its Derived Compounds. XVII. A Synthesis of Syringaldehyde from Vanillin

Pearl,Irwin;Beyer,Donald

J.Am.Chem.Soc.
Vol.74(17) 1952 pp.4262-4263
DOI: 10.1021/ja01137a006

No Abstract

Microscale Reactions of Vanillin

Pearl,Irwin

J.Chem.Educ.
Vol.69(2) 1992 p.A43-
DOI: 10.1021/ed069pA43

Abstract

In this paper five microscale experiments which allow first-year organic student sot study the properties and reactions of vanillin are presented.

Evilblaze · « **Reply #99 on:** May 11, 2011, 01:16:36 PM »

Synthesen von Indolen mit (2-Aminoäthyl)-, (2-Aminopropyl)-oder Alkanolamin-Seitenketten am Sechsring. 5. Mitt. über synthetische Indol-Verbindungen [1]
F. Troxler
Helvetica Chimica Acta Volume 51, Issue 7, pages 1616–1628, 31 October 1968 DOI: 10.1002/hlca.19680510717

Studies in the indole series. Part I. Indolylalkylamines
B. Heath-Brown and P. G. Philpott
J. Chem. Soc., 1965, 7165-7178 DOI: 10.1039/JR9650007165

Studies in the indole series. Part II. Indolylalkylhydroxylamines
A. Cohen and B. Heath-Brown
J. Chem. Soc., 1965, 7179-7184 DOI: 10.1039/JR9650007179

Studies in the indole series. Part III. The Japp–Klingemann reaction
B. Heath-Brown and P. G. Philpott
J. Chem. Soc., 1965, 7185-7193 DOI: 10.1039/JR9650007185

Conversion of indolylalkylhydroxylamines to stimulant amines in vivo
A.W. Lessina
Biochemical Pharmacology Volume 15, Issue 4, April 1966, Pages 481-487 doi:10.1016/0006-2952(66)90258-9

Hallucinogens as discriminative stimuli: A comparison of 4-OMe and 5-OMe DMT with their methylthio counterparts
R.A. Glennon
Life Sciences Volume 30, Issue 5, 1 February 1982, Pages 465-467 doi:10.1016/0024-3205(82)90463-5

Author Topic: 2011 Reference Requests (Read 3668 times)

Shake

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